pd_meltingpoint:≥170oC
Appearance:White to Off-White Crystalline Powder
Purity:99%
Quality products make an important contribution to long-term revenue and profitability. Buy Good Supplier In China Methoxydienone 2322-77-2 Offer
Max LMG is a progestin derived steroid and not a 17-alpha alkylated steroid. Max LMG is structurally related to RU-486 and acts as an antiprogesterone, decreasing estrogen-like effects.
This substance is used in formulation or re-packing,at industrial sites and in manufacturing.
dl-3-methoxy-13β-ethylgona-2,5(10)-dien-17β-ol
dl-3-methoxy-13β-ethylgona-2,5(10)-dien-17-one
Conditions | Yield |
---|---|
With molecular sieve; aluminum isopropoxide; butanone; In benzene;
|
76% |
With cyclohexanone; aluminum isopropoxide; In toluene; Heating;
|
2-Ethyl-3-vinyl-cyclopentanone
dl-3-methoxy-13β-ethylgona-2,5(10)-dien-17-one
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps
1: 80 percent NaH, Et3N / 1,2-dimethoxy-ethane; paraffin / 1.) 3.5 h, reflux; 2.) 40 min
2: 1.) 2,4,6-trimethylphenol, pyridine; 2.) oxalic acid / 1.) methylcyclohexane, 13.5 h, 98 deg C, irradiation
3: 99 percent / LiAlH4 / diethyl ether
4: 62 percent / K, aniline, NH3 / tetrahydrofuran / 1 h
5: 76 percent / 2-butanone, aluminium isopropylate, mol. sieve / benzene
With pyridine; lithium aluminium tetrahydride; molecular sieve; Mesitol; ammonia; oxalic acid; aluminum isopropoxide; sodium hydride; triethylamine; aniline; butanone; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; paraffin; benzene;
|
|
Multi-step reaction with 6 steps
1: 86 percent / TsOH*H2O / 14 h / Heating
2: 1.) 1.3 M MeLi; 2.) 10 percent H2SO4 / 1.) Et2O, 0.5 h; -20 deg C, 3h; 2.) Et2O, 14 h, RT
3: 1.) 2,4,6-trimethylphenol, pyridine; 2.) oxalic acid / 1.) methylcyclohexane, 13.5 h, 98 deg C, irradiation
4: 99 percent / LiAlH4 / diethyl ether
5: 62 percent / K, aniline, NH3 / tetrahydrofuran / 1 h
6: 76 percent / 2-butanone, aluminium isopropylate, mol. sieve / benzene
With pyridine; lithium aluminium tetrahydride; molecular sieve; Mesitol; sulfuric acid; ammonia; methyllithium; oxalic acid; aluminum isopropoxide; toluene-4-sulfonic acid; aniline; butanone; In tetrahydrofuran; diethyl ether; benzene;
|
|
Multi-step reaction with 5 steps
1: 1.) NaH, 2.) H2SO4 / 1.) DME, paraffin oil; Et2O; 2.) MeOH
2: 1.) 2,4,6-trimethylphenol, pyridine; 2.) oxalic acid / 1.) methylcyclohexane, 13.5 h, 98 deg C, irradiation
3: 99 percent / LiAlH4 / diethyl ether
4: 62 percent / K, aniline, NH3 / tetrahydrofuran / 1 h
5: 76 percent / 2-butanone, aluminium isopropylate, mol. sieve / benzene
With pyridine; lithium aluminium tetrahydride; molecular sieve; Mesitol; sulfuric acid; ammonia; oxalic acid; aluminum isopropoxide; sodium hydride; aniline; butanone; In tetrahydrofuran; diethyl ether; benzene;
|
The CAS number of Methoxydienone is 2322-77-2.
More information of Methoxydienone 2322-77-2 are:
CAS Number |
2322-77-2 |
Density |
1.09 g/cm3 |
Melting Point |
≥170oC |
Boiling Point |
448 °C at 760 mmHg |
Flash Point |
188.8 °C |
Vapor Pressure |
3.21E-08mmHg at 25°C |
Refractive Index |
1.551 |
PSA |
26.30000 |
LogP |
4.80260 |
Synonyms for Methoxydienone 2322-77-2:METHOXYDIENONE;13-beta-Ethyl-3-methoxygona-2,5(10)-dien-17-one;(8r,9s,13s,14s)-13-ethyl-3-methoxy-4,6,7,8,9,11,12,14,15,16-decahydro-1h-cyclopenta[a]phenanthren-17-one;13-Ethyl-3-methoxy-gona-2,5(10;D(-)-18-METHYL-3-METHOXY-ESTRA-2,5(10)-DIEN-17-ONE;METHOXYDIENONE(13-BETA-ETHYL-3-METHOXYGONA-2,5(10)-DIEN-17-ONE);18-Methylestra-2,5(10)-dien-3-ol-17-one-3-methy ether;3-Methoxy-18-methylestra-2,5(10)-dien-17-one
The chemical formula of Methoxydienone is C20H28O2 which containing 20 Carbon atoms,28 Hydrogen atoms and 2 Oxygen atoms,and the molecular weight of Methoxydienone is 300.441.
InChI:InChI=1/C20H28O2/c1-3-20-11-10-16-15-7-5-14(22-2)12-13(15)4-6-17(16)18(20)8-9-19(20)21/h5,16-18H,3-4,6-12H2,1-2H3/t16-,17-,18+,20+/m1/s1
Relevant articles related to Methoxydienone:
Article |
Source |
Total synthesis with a chirogenic opening move demonstrated on steroids with estrane or 18a-homoestrane skeleton |
Quinkert,Del Grosso,Doring,Doring,Schenkel,Bauch,Dambacher,Bats,Zimmermann,Durner , p. 1345 - 1391 (2007/10/02) |
Total-synthesis of (-)-norgestrel |
Baier,Durner,Quinkert , p. 1054 - 1068 (2007/10/02) |
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