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pd_meltingpoint:181-186 °C
Appearance:White powder
Purity:99%
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4-Methoxybenzoic acid (p-Anisic acid) is used in oxidation and reduction of cytochrome c in solution through different self-assembled monolayers on gold electrodes using cyclic voltammetry. p-Anisic acid has antiseptic properties. It is also used as an intermediate in the preparation of more complex organic compounds.
1-(4-methoxyphenyl)ethanone
4-methoxybenzoic acid
| Conditions | Yield |
|---|---|
|
With copper(II) nitrate trihydrate; oxygen; In acetonitrile; at 120 ℃; for 10h; under 4500.45 Torr; Autoclave;
|
99% |
|
With oxygen; copper(II) nitrate; In acetonitrile; at 120 ℃; for 10h; under 4500.45 Torr;
|
99% |
|
With copper(l) iodide; hydroxylamine hydrochloride; oxygen; In dimethyl sulfoxide; at 100 ℃; for 8h; Solvent; Reagent/catalyst; Temperature;
|
95% |
|
With 1,10-Phenanthroline; oxygen; copper diacetate; potassium hydroxide; In dimethyl sulfoxide; at 130 ℃; for 12h; under 3000.3 Torr; Autoclave;
|
95% |
|
1-(4-methoxyphenyl)ethanone; With iodine; dimethyl sulfoxide; In chlorobenzene; at 130 ℃; for 3h;
With tert.-butylhydroperoxide; In chlorobenzene; at 20 - 130 ℃; for 3h; Time;
|
94% |
|
With hydroxylamine hydrochloride; iodine; In dimethyl sulfoxide; at 100 ℃; for 4h;
|
93% |
|
With sodium hypochlorite; lithium hypochlorite; In ethanol; at 77 ℃; for 2h;
|
92% |
|
With Iron(III) nitrate nonahydrate; iodine; oxygen; dimethyl sulfoxide; at 130 ℃; for 12h; under 750.075 Torr; Sealed tube; Green chemistry;
|
92% |
|
With Iron(III) nitrate nonahydrate; iodine; oxygen; In dimethyl sulfoxide; at 130 ℃; for 12h; Sealed tube;
|
92% |
|
With Oxone; trifluoroacetic acid; In 1,4-dioxane; for 10h; Reflux; Green chemistry;
|
90% |
|
With iodine; dimethyl sulfoxide; copper(II) oxide; at 90 ℃; for 3h;
|
88% |
|
With carbon tetrabromide; oxygen; In ethyl acetate; for 12h; Irradiation;
|
87% |
|
1-(4-methoxyphenyl)ethanone; With tert.-butylhydroperoxide; sodium hydroxide; tungsten(VI) oxide; In water; at 80 ℃; for 8h;
With hydrogenchloride; In water;
|
85% |
|
With oxygen; manganese (II) acetate tetrahydrate; cobalt(II) diacetate tetrahydrate; In acetic acid; at 100 ℃; for 15h; under 760.051 Torr;
|
84% |
|
With sodium percarbonate; potassium tert-butylate; sphingosylphosphorylcholine; meta-dinitrobenzene; In tert-butyl alcohol; at 80 ℃; for 5h;
|
58% |
|
With meta-dinitrobenzene; sodium hydroxide; In water; at 100 ℃; for 2.5h; Sealed tube;
|
56.2% |
|
With tert.-butylhydroperoxide; rhenium(VII) oxide; acetic acid; at 100 ℃; for 4.5h;
|
55% |
|
1-(4-methoxyphenyl)ethanone; With aluminum (III) chloride; N,N-dimethyl-aniline; In toluene; at 100 - 110 ℃; for 2 - 3h;
With hydrogenchloride; water; at 20 ℃; pH=1 - 2; Product distribution / selectivity;
|
15% |
|
With Amberlyst 15; In toluene; for 32h; Reflux;
|
10% |
|
With sodium hydroxide; chlorine;
|
|
|
With 18-crown-6 ether; acetophenone; In benzene; at 25 ℃; for 24h; Mechanism; relative reactivity; further oxidative agents;
|
|
|
With sodium hydroxide; potassium chloride; potassium hexacyanoferrate(III); In methanol; water; at 30 ℃; Kinetics; further temperature;
|
|
|
With manganese(II) nitrate; oxygen; cobalt(II) nitrate; In acetic acid; at 100 ℃; for 6h;
|
|
|
With copper(II) choride dihydrate; oxygen; lithium bromide; tert-butyl alcohol; at 130 ℃; for 10h; under 7500.75 Torr; Reagent/catalyst; Autoclave; Green chemistry;
|
|
|
With dihydrogen peroxide; In water; at 22 - 25 ℃; for 11688h;
|
|
|
Multi-step reaction with 2 steps
1: iodine; dimethyl sulfoxide / chlorobenzene / 120 °C
2: tert.-butylhydroperoxide / 6 h
With tert.-butylhydroperoxide; iodine; dimethyl sulfoxide; In chlorobenzene;
|
anethole
4-methoxy-benzaldehyde
4-methoxybenzoic acid
| Conditions | Yield |
|---|---|
|
durch elektrolytische Oxydation in neutraler, saurer oder alkalischer waessriger Suspension;
|
The CAS number of Anisic acid is 100-09-4.
More information of Anisic acid 100-09-4 are:
|
CAS Number |
100-09-4 |
|
Density |
1.208 g/cm3 |
|
Melting Point |
181-186 °C |
|
Boiling Point |
278.305 °C at 760 mmHg |
|
Flash Point |
115.46 °C |
|
Vapor Pressure |
0.002mmHg at 25°C |
|
Refractive Index |
1.571-1.576 |
|
HS CODE |
2918.90 DERIVATION |
|
PSA |
46.53000 |
|
LogP |
1.39340 |
|
Pka |
4.50(at 25℃) |
|
Previous Years |
2001, SPECIFICATIONS WILL BE CONSIDERED AT JECFA 59. O2001, SPECIFICATIONS WILL BE CONSIDERED AT JECFA 59. O |
Synonyms for Anisic acid 100-09-4:p-Anisicacid (6CI,7CI,8CI);4-Anisic acid;4-Methoxybenzoic acid;Draconicacid;NSC 32742;NSC 7926;p-Methoxybenzoic acid;
The chemical formula of Anisic acid is C8H8O3 which containing 8 Carbon atoms,8 Hydrogen atoms and 3 Oxygen atoms,and the molecular weight of Anisic acid is 152.15.
4-methoxybenzoic acid, also known as p-Anisic acid or draconic acid, is an organic acid with a sweet flavor. It is one of the isomers(m-anisic acid, and o-anisic acid) of anisic acid. The term "anisic acid" often refers to this form specifically. P-anisic acid is produced through the oxidation of p-cresyl-methyl ether.
InChI:InChI=1/C8H8O3/c1-11-7-4-2-6(3-5-7)8(9)10/h2-5H,1H3,(H,9,10)
Relevant articles related to Anisic acid:
|
Article |
Source |
|
Lithium hypochlorite-clorox as a novel oxidative mixture for methyl ketones and methyl carbinols |
Madler,Klucik,Soell,Brown,Liu,Berlin,Benbrook,Birckbichler,Nelson , p. 230 - 234 (1998) |
|
- |
Callow,Hill , p. 844,847 (1937) |
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