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Purity:99%
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Organic synthesis intermediates.
phenylacetyl chloride
diethyl malonate
diethyl 2-(2-phenylacetyl)malonate
Conditions | Yield |
---|---|
diethyl malonate; With ethanol; magnesium; In tetrachloromethane; toluene; for 1h; Heating;
phenylacetyl chloride; In tetrachloromethane; toluene; at 20 ℃; for 1h;
|
90% |
With chloroform; magnesium;
|
|
With magnesium;
|
|
With sodium;
|
|
Multistep reaction; (i) Mg, EtOH, (ii) /BRN= 742254/;
|
|
diethyl malonate; With triethylamine; magnesium chloride; In acetonitrile; at 0 ℃; for 0.5h; Inert atmosphere;
phenylacetyl chloride; In acetonitrile; at 20 ℃;
|
|
With magnesium; In ethanol; toluene; at 80 ℃;
|
|
diethyl malonate; With sodium hydride; In tetrahydrofuran; for 1h;
phenylacetyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;
|
489 mg |
ethanol
2,2-dimethyl-5-(2-phenylacetyl)-1,3-dioxane-4,6-dione
diethyl 2-(2-phenylacetyl)malonate
Conditions | Yield |
---|---|
for 3h; Reflux;
|
The CAS number of Diethyl(phenylacetyl)malonate is 20320-59-6.
More information of Diethyl(phenylacetyl)malonate 20320-59-6 are:
CAS Number |
20320-59-6 |
Density |
1.148±0.06 g/cm3(Predicted) |
Boiling Point |
120 °C(Press: 0.01 Torr) |
HS CODE |
2918300090 |
PSA |
69.67000 |
LogP |
1.54060 |
Pka |
8.76±0.59(Predicted) |
Synonyms for Diethyl(phenylacetyl)malonate 20320-59-6:phenylacetyl-malonic acid diethyl ester;Phenylacetyl-malonsaeure-diaethylester;Phenylacetylmalonsaeurediethylester;Phenylacetylmalonic acid ethylester;
The chemical formula of Diethyl(phenylacetyl)malonate is C15H18O5 which containing 15 Carbon atoms,18 Hydrogen atoms and 5 Oxygen atoms,and the molecular weight of Diethyl(phenylacetyl)malonate is 278.305.
Relevant articles related to Diethyl(phenylacetyl)malonate:
Article |
Source |
The Interrupted Pummerer Reaction in a Sulfoxide-Catalyzed Oxidative Coupling of 2-Naphthols |
He, Zhen,Pulis, Alexander P.,Procter, David J. supporting information, p. 7813 - 7817 (2019/05/15) |
Novel Inhibitors of Hepatitis C Virus Replication |
- Page/Page column 52-53, (2009/10/21) |
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